Rutz Josiane K, Borges Caroline D, Zambiazi Rui C, Crizel-Cardozo Michele M, Kuck Luiza S, Noreña Caciano P Z
Department of Agroindustrial Science and Technology, Federal University of Pelotas, Pelotas, RS, Brazil.
Center of Chemical, Pharmaceuticals and Food Sciences, Federal University of Pelotas, Pelotas, RS, Brazil.
Food Chem. 2017 Apr 1;220:59-66. doi: 10.1016/j.foodchem.2016.09.194. Epub 2016 Sep 30.
This study aimed at microencapsulating palm oil, containing high carotenoid content, with chitosan/xanthan and chitosan/pectin, using the complex coacervation method, followed by atomization and lyophilization. The DSC technique was used to confirm the encapsulation. The atomized microparticles had spherical shape and irregular size, and the lyophilized microparticles had irregular shape and size. Lyophilization resulted in lower carotenoids losses, and higher yield and encapsulation efficiency. In addition, the release profile in both water and gastrointestinal fluid was satisfactory. Prior to their application in food, a greater percentage of carotenoids was released in the fluid that simulates gastrointestinal conditions; however, the compounds were degraded after their release. In this case, the chitosan/pectin microparticles showed the best release profile. After processing, the release was lower and the released compounds were not degraded. Thus, the chitosan/xanthan microparticles showed the best potential for practical application, particularly, in yogurt preparation.
本研究旨在采用复凝聚法,用壳聚糖/黄原胶和壳聚糖/果胶对富含高类胡萝卜素的棕榈油进行微囊化,随后进行雾化和冻干。采用差示扫描量热法(DSC)技术确认包封情况。雾化后的微粒呈球形但尺寸不规则,冻干后的微粒形状和尺寸均不规则。冻干导致类胡萝卜素损失较低,产率和包封效率较高。此外,在水和胃肠液中的释放曲线均令人满意。在将其应用于食品之前,在模拟胃肠条件的液体中释放出更大比例的类胡萝卜素;然而,这些化合物在释放后会降解。在这种情况下,壳聚糖/果胶微粒显示出最佳的释放曲线。加工后,释放量较低且释放出的化合物未降解。因此,壳聚糖/黄原胶微粒在实际应用中显示出最佳潜力,特别是在酸奶制备中。