Karydas Andreas Germanos, Czyzycki Mateusz, Leani Juan José, Migliori Alessandro, Osan Janos, Bogovac Mladen, Wrobel Pawel, Vakula Nikita, Padilla-Alvarez Roman, Menk Ralf Hendrik, Gol Maryam Ghahremani, Antonelli Matias, Tiwari Manoj K, Caliri Claudia, Vogel-Mikuš Katarina, Darby Iain, Kaiser Ralf Bernd
Nuclear Science and Instrumentation Laboratory, International Atomic Energy Agency (IAEA) Laboratories, A-2444 Seibersdorf, Austria.
AGH University of Science and Technology, Faculty of Physics and Applied Computer Science, Al. A. Mickiewicza 30, 30-059 Krakow, Poland.
J Synchrotron Radiat. 2018 Jan 1;25(Pt 1):189-203. doi: 10.1107/S1600577517016332.
The International Atomic Energy Agency (IAEA) jointly with the Elettra Sincrotrone Trieste (EST) operates a multipurpose X-ray spectrometry endstation at the X-ray Fluorescence beamline (10.1L). The facility has been available to external users since the beginning of 2015 through the peer-review process of EST. Using this collaboration framework, the IAEA supports and promotes synchrotron-radiation-based research and training activities for various research groups from the IAEA Member States, especially those who have limited previous experience and resources to access a synchrotron radiation facility. This paper aims to provide a broad overview about various analytical capabilities, intrinsic features and performance figures of the IAEA X-ray spectrometry endstation through the measured results. The IAEA-EST endstation works with monochromatic X-rays in the energy range 3.7-14 keV for the Elettra storage ring operating at 2.0 or 2.4 GeV electron energy. It offers a combination of different advanced analytical probes, e.g. X-ray reflectivity, X-ray absorption fine-structure measurements, grazing-incidence X-ray fluorescence measurements, using different excitation and detection geometries, and thereby supports a comprehensive characterization for different kinds of nanostructured and bulk materials.
国际原子能机构(IAEA)与的里雅斯特埃莱特拉同步加速器(EST)合作,在X射线荧光光束线(10.1L)上运营一个多用途X射线光谱终端站。自2015年初以来,该设施通过EST的同行评审程序向外部用户开放。利用这一合作框架,IAEA为其成员国的各个研究小组支持和促进基于同步辐射的研究和培训活动,特别是那些以前接触同步辐射设施的经验和资源有限的小组。本文旨在通过测量结果,对IAEA X射线光谱终端站的各种分析能力、固有特性和性能指标进行全面概述。IAEA-EST终端站在电子能量为2.0或2.4 GeV的埃莱特拉储存环中,使用能量范围为3.7-14 keV的单色X射线工作。它提供了不同先进分析探针的组合,例如X射线反射率、X射线吸收精细结构测量、掠入射X射线荧光测量,采用不同的激发和检测几何结构,从而支持对不同种类的纳米结构材料和块状材料进行全面表征。