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超声复合环境下高压水热溶胶-凝胶法制备 TiO/CNT 介孔纳米材料的物理化学和抗菌评价。

Physicochemical and Antibacterial Evaluation of TiO/CNT Mesoporous Nanomaterials Prepared by High-Pressure Hydrothermal Sol-Gel Method under an Ultrasonic Composite Environment.

机构信息

Sino-French Institute of Nuclear Engineering and Technology, Sun Yat-Sen University, Zhuhai 519082, China.

School of Chemical Engineering and Technology, Sun Yat-Sen University, Zhuhai 519082, China.

出版信息

Molecules. 2023 Apr 3;28(7):3190. doi: 10.3390/molecules28073190.

Abstract

TiO has attracted significant research interest, principally due to its nontoxicity, high stability, and abundance. Carbon-doped TiO can improve light absorption efficiency. In order to prepare high-efficiency photocatalysts, carbon-doped composites were prepared by hydrothermal reaction in a high-pressure reactor, and then TiO/CNT mesoporous composites were prepared by the sol-gel method in an ultrasonic environment. Characterized by SEM and TEM, the composite materials contained TiO nanoparticles as well as CNT. After phase analysis, it was the anatase-doped phase. The following infrared light absorption performance and bactericidal performance tests showed that it had better infrared and visible light absorption performance than pure TiO. The TiO/CNT mesoporous nanomaterials synthesized in this work are possible for clean industrial productions.

摘要

TiO 引起了广泛的研究兴趣,主要是因为它的无毒、高稳定性和丰富性。碳掺杂的 TiO 可以提高光吸收效率。为了制备高效光催化剂,采用高压釜水热反应法制备了碳掺杂复合材料,然后在超声环境下通过溶胶-凝胶法制备了 TiO/CNT 介孔复合材料。采用 SEM 和 TEM 对复合材料进行了表征,复合材料中含有 TiO 纳米粒子和 CNT。经过物相分析,掺杂相为锐钛矿相。随后的红外光吸收性能和杀菌性能测试表明,它比纯 TiO 具有更好的红外和可见光吸收性能。本工作中合成的 TiO/CNT 介孔纳米材料有望用于清洁工业生产。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/654e/10095998/1bafd1358162/molecules-28-03190-sch001.jpg

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